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Batch Rotary Kiln

Precursor powders of y 1 ba 2 cu 3 o 6x 123 derived from spray roasting were calcined in a batch rotary kiln.The optimum conditions were 15 min in air at temperatures between 920 and 940c for 1.5 vol solid loading.Pure 123 was formed in a single calcination step from homogeneous, micrometersized precursor material containing y 2 o 3, cuo, and baco 3.

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